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Waters

Connecting the nitrogen exhaust line

Article number: 208264

Required materials

  • Chemical-resistant, powder-free gloves
  • Utility knife
  • Nitrogen exhaust trap bottle
  • 4-mm PTFE tubing and 12-mm PTFE tubing (included in the SELECT SERIES MRT installation kit)

To connect the nitrogen exhaust line:

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Warning: To avoid exposure to toxic solvent vapor:

  • The source exhaust line supplied with the system must be fed into a ducted laboratory fume hood or connected to a laboratory exhaust system. The laboratorY exhaust system must be capable of supporting a gas load of 2000 L/hour.
  • The pressure within the laboratory exhaust must be less than atmospheric pressure, but not less than -10 mbar gauge, while under gas load.
  • When running an LC with a high aqueous flow (≥ 60% water at ≥ 0.5 mL/min), liquid solvent may condense and accumulate in the laboratory exhaust system, in which case, Waters recommends that the exhaust system include the capability to drain off any solvent accumulation, or that the exhaust system is designed to prevent condensation, for example, by being open and maintaining a gas flow of at least 5000 L/hour through the exhaust system.

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Warning: To avoid personal contamination with biologically hazardous, toxic, and corrosive materials, wear chemical-resistant, powder-free gloves when performing this procedure.

Notice: To prevent serious damage to the instrument, two separate exhaust systems are required: one for nitrogen, the other for the roughing pumps. Vent the exhausts to atmosphere through separate lines. Oil mist can seriously damage the instrument if the nitrogen exhaust line connects with the roughing pump exhaust line. Your warranty does not cover damage caused by routing exhaust lines incorrectly.

  1. Locate the nitrogen exhaust trap bottle in an accessible area below the instrument.
Figure 1: Nitrogen exhaust trap bottle

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clipboard_eb9bc69ad06380e65b58194e30fa773bd.png Notice: To avoid gas leaks, use the tube cutter to cut the PTFE tubing squarely.

  1. Cut a length of 4-mm tubing long enough to connect the instrument to the nitrogen exhaust trap bottle.
  2. Connect one end of the tubing to the pilot valve port on the instrument’s rear panel.
  3. Connect the free end of the tubing to the pilot valve port on the nitrogen exhaust trap bottle.
  4. Cut a length of 12-mm tubing long enough to connect the instrument to the nitrogen exhaust trap bottle.
  5. Connect one end of the tubing to the exhaust port on the instrument’s rear panel.
  6. Connect the free end of the tubing to the inlet port on the nitrogen exhaust trap bottle.

clipboard_ef4ffd808ab7204f950a298a7f8239a76.png Notice: To avoid gas leaks, use the tube cutter to cut the PTFE tubing squarely.

  1. Cut a second length of 12-mm tubing long enough to connect the nitrogen exhaust trap bottle to the exhaust vent.
  2. Insert one end of the tubing into the outlet port on the nitrogen exhaust trap bottle.
  3. Route the free end of the tubing to the exhaust vent.

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