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Waters

No peaks eluting from the GC column when using APGC - WKB114229

Article number: 114229

SYMPTOMS

  • No peaks elute from column 
  • Complete noise background; no bleed peaks come off
  • Cone gas set to 0 in order to elevate any background peaks (should be between 100 and 150 in stepwave instrument)
  • Peaks ionizing the heptacosa in background 
  • All other source conditions tuned normally 

ENVIRONMENT

  • APGC
  • UNIFI
  • Xevo G2-XS
  • Xevo G2-S
  • Xevo TQ-S
  • Xevo TQ-XS
  • SYNAPT G2
  • SYNAPT G2-S 
  • SYNAPT G2-Si

CAUSE

Broken column (column snapped in the middle)

FIX or WORKAROUND

Swap columns

ADDITIONAL INFORMATION

 

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