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For ACQUITY UPLC Sample Manager, Characterize needle and loop volumes fails to calibrate system volume - WKB81497

Article number: 81497

SYMPTOMS

  • Tailing peaks
  • Characterize needle and loop volumes: failed to calibrate system volume
  • All diagnostic tests pass

ENVIRONMENT

  • ACQUITY UPLC Sample Manager
  • ACQUITY I-CLASS SM-FL

CAUSE

The ferrule and backing ferrule on the sample loop are not installed correctly or the injector pod has a leak

FIX or WORKAROUND

  1. Replace the sample loop.
  2. Rerun the test.
  3. If it continues to fail replace the injector valve

ADDITIONAL INFORMATION


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